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Hello Ian,
I think you have an intel controller on that board and that is actually the one I would setup your raid on.
A basic out line would be as follows
boot into bios and enable intel raid ( after making sure you are plugged into SATA 1 and 2 )
F10 to save and exit bios
Make sure you have your intel raid drivers on a floppy you made from your mobo disk
upon rebooting hit CTRL I to enter the intel raid utility
follow prompts to setup your raid 0
insert your XP cd and once it boots and starts the install process look out for the F6 prompt and this will enable you to install the Intel raid drivers from your floppy
continue with XP install and once done install your chipset drivers and intel raid utility and the rest of your required drivers
That is a basic out line
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